HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylsulphonyl isocyanate → HCID 22764598, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylsulphonyl isocyanate | HCID 76096 | — |
| Reactant | 3-Amino-5,6-dimethyl-1,2,4-triazine | HCID 87163 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22764598 | HCID 22764598 | — |
Reaction Steps
To a dry, well stirred mixture of 6 g of 3-amino-5,6-dimethyl-1,2,4-triazine in 100 ml of methylene chloride at ambient temperature and pressure was added 9 g of benzenesulfonyl isocyanate. The mixture was stirred for 4 hours and the precipitated product removed by filtration. After washing with 1-chlorobutane, the product melted at 155°-158°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120691 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-a775ad6a09dc4dc4a0f896fc1945c24a |
| Source note | uspto-grants-1978_10 |