HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Phenol, 4-(heptafluoropropyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12294033 | HCID 12294033 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Phenol, 4-(heptafluoropropyl)- | HCID 12294034 | 92% |
Reaction Steps
A solution of p-C3F7C6H4OC(O)CH3 (33.2 g; 0.14 mole) in CH3OH (200 ml) containing concentrated HCl (20 ml) was heated to reflux for 24 hours. After cooling and aspiration of the solvent, a brown liquid resulted (28.4 g; 99% crude yield). A gas chromatographic analysis indicated primarily one major component. Distillation provided the product p-C3F7C6H4OH (26.2 g; 92% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120863 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-3e1fbe057ed1442181fac9be62c5b130 |
| Source note | uspto-grants-1978_10 |