HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 3-(2-Chloroethanesulfonyl)-N-[2-(ethenylsulfanyl)ethyl]propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Chloroethanesulfonyl)propanoyl chloride | HCID 13668397 | — |
| Reactant | HCID 14979952 | HCID 14979952 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-(2-Chloroethanesulfonyl)-N-[2-(ethenylsulfanyl)ethyl]propanamide | HCID 22765149 | — |
Reaction Steps
A solution of 5.92 g 3-(2-chloroethylsulphonyl)-propionyl chloride in 75 ml dichloromethane was treated dropwise with a solution of 2.65 g 2-vinylthioethylamine and 2.6 g triethylamine in dichlormethane. After 2 hours, the solution was evaporated and the residue recrystallised from aqueous ethanol. Yield 6.1 g; Mp. 102° to 103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120898 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-6ce456efd65440eb8daf4be7e6766374 |
| Source note | uspto-grants-1978_10 |