HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 22765157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Chloroethanesulfonyl)-N-[2-(ethenylsulfanyl)ethyl]propanamide | HCID 22765149 | — |
| Product | HCID 22765157 | HCID 22765157 | — |
Reaction Steps
0.8 g Triethylamine was added to a solution of 2.0 g Intermediate 2 in 10 ml dimethylformamide. After stirring 1 hour the mixture was filtered and the filtrate evaporated. The residue was recrystallised form ethyl acetate and then from dichloromethanepetrolether. Yield 1.1 g; Mp. 93° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120898 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-4b5f9f2540a346feb6e9abd33c727aa9 |
| Source note | uspto-grants-1978_10 |