Sodium Carbonate → HCID 22712554, compound

HRID 1112212Notes

Reaction equation

HRID 1112212 reaction equation
Cl.[CH3:2][C:3]1[NH:7][CH:6]=[N:5][C:4]=1[CH2:8][S:9][CH2:10][CH2:11][S:12][C:13](=[S:16])[NH:14][CH3:15].C(=O)([O-])[O-].[Na+].[Na+]>>[CH3:15][NH:14][C:13](=[S:16])[S:12][CH2:11][CH2:10][S:9][CH2:8][C:4]1[N:5]=[CH:6][NH:7][C:3]=1[CH3:2]

Participants

3

Reactant 2

HCID 10340Sodium CarbonateHCID 887953812-(5-methyl-4-imidazolylmethylthio)ethyl-N-methyldithiocarbamate hydrochloride

Product 1

HCID 22712554HCID 22712554, compound

Procedure

This hydrochloride may be treated with aqueous sodium carbonate and the mixture extracted with chloroform and the chloroform extracts evaporated to give the free base.

Workup

  1. extractionthe mixture extracted with chloroform
  2. customthe chloroform extracts evaporated
  3. customto give the free base

Sources & evidence

ORD record
ord-62c02394cffd4daaacb8b90080fd6789
Source dataset
uspto-grants-1978_10
Patent number
US04120966

Reaction notes

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