HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-((4-Methyl-5-imidazolyl)methylthio)ethylthiourea → HCID 178433689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-((4-Methyl-5-imidazolyl)methylthio)ethylthiourea | HCID 12718697 | — |
| Reactant | 4-{[(2-Chloroethyl)sulfanyl]methyl}-5-methyl-1H-imidazole | HCID 13217360 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178433689 | HCID 178433689 | — |
Reaction Steps
1-Chloro-2-(5-methyl-4-imidazolylmethylthio)ethane and N-[2-(5-methyl-4-imidazolylmethylthio)ethyl]thiourea are heated together at reflux temperature in ethanol, and the mixture is evaporated and the residue purified to give the title compound, which may be converted into a suitable salt by ion-exchange chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120966 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-400d7b5f0755453094872018afe7c12d |
| Source note | uspto-grants-1978_10 |