HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl Isocyanate → methyl 4-(p-chlorophenyl)-N-methoxycarbonylallophanimidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| Reactant | N-carbomethoxy-O-methylisourea | HCID 53429793 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | methyl 4-(p-chlorophenyl)-N-methoxycarbonylallophanimidate | HCID 54018948 | — |
Reaction Steps
To 13 parts of this methyl N-(1-amino-1-methoxymethylene)carbamate, m.p. 36°-39.5° in 140 parts of methylene chloride is added 15 parts of 4-chlorophenyl isocyanate. The reaction mixture is stirred overnight and the solution filtered to give 10 parts of methyl 4-(4-chlorophenyl)-N-methoxycarbonylallophanimidate melting at 170° dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04121921 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-09c811fd3b18416f9e5171b61a975288 |
| Source note | uspto-grants-1978_10 |