HRID1112362

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6417

2,2-Dimethylpropanoic acid

C5H10O2

结构：CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42

HCID71204

Methyl (3alpha,16alpha)-eburnamenine-14-carboxylate

C21H24N2O2

2 次

PRODUCTS

生成物

结构：CC(C)(C)C(=O)[O-].CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42

HCID86736086

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

According to the method of the preceding example, 4 g of the salt are prepared starting from 1.02 g of pivalic acid and 3.36 g of apovincamine. The product has melting point of 110° C., is insoluble in water and soluble in alcohol; the apovincamine content thereof is 73.8%.

WORKUP

后处理

customare prepared