HRID1112363

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID18189

4-Acetamidobutyric acid

C6H11NO3

结构：CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42

HCID71204

Methyl (3alpha,16alpha)-eburnamenine-14-carboxylate

C21H24N2O2

2 次

PRODUCTS

生成物

结构：CC(=O)NCCCC(=O)[O-].CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42

HCID86736087

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

According to the method of the preceding example, there are obtained, starting from 3.36 g of apovincamine and 1.45 g of 4-acetamidobutyric acid, 4.4 g of a product, having melting point of 128° C. and insoluble in water and alcohol. The apovincamine content of the salt is 56%.

WORKUP

后处理

customare obtained