HRID1112368

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6497

Dimethyl sulfate

C2H6O4S

结构：CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42

HCID71204

Methyl (3alpha,16alpha)-eburnamenine-14-carboxylate

C21H24N2O2

PRODUCTS

生成物

结构：CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42.COS(=O)(=O)[O-]

HCID86736091

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

7.3 g of salt are prepared, likewise the preceding example, starting from 6.73 g (2.10-2 moles) of apovincamine and from about 2 mls of dimethyl sulfate. The final product has a melting point of 280° C. and is water soluble but poorly soluble in alcohol.