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HRID1112370

反应详情

EQUATION

反应方程式

HRID 1112370 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)COc1ccc(Cl)cc1
HCID26229

4-Chlorophenoxyacetic acid

C8H7ClO3

结构：CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42
HCID71204

Methyl (3alpha,16alpha)-eburnamenine-14-carboxylate

C21H24N2O2

2 次

PRODUCTS

生成物

1
结构：CC[C@@]12C=C(C(=O)OC)n3c4c(c5ccccc53)CCN(CCC1)[C@H]42.O=C([O-])COc1ccc(Cl)cc1
HCID86736093

未命名化合物

收率 76.9%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

4 g of the salt are prepared, according to the method of the example 19.a, starting from 3.36 g of apovincamine and 1.86 g of p-chlorophenoxyacetic acid. The melting point of the salt is about 120° C. and it is insoluble in water; the content of apovincamine is 64%.

WORKUP

后处理

  1. customis about 120° C.