Decanoic Acid → HCID 86736098, compound

HRID 1112375Notes

Reaction equation

HRID 1112375 reaction equation
[CH3:1][CH2:2][C@:3]12[CH:19]=[C:18]([C:20]([O:22][CH3:23])=[O:21])[N:17]3[C:9]4=[C:10]([CH2:24][CH2:25][N:7]([C@@H:8]14)[CH2:6][CH2:5][CH2:4]2)[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=13.[OH:26][C:27]([CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])=[O:28]>O>[CH3:1][CH2:2][C@:3]12[CH:19]=[C:18]([C:20]([O:22][CH3:23])=[O:21])[N:17]3[C:9]4=[C:10]([CH2:24][CH2:25][N:7]([C@@H:8]14)[CH2:6][CH2:5][CH2:4]2)[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=13.[O-:28][C:27]([CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])=[O:26]

Participants

4

Reactant 2

HCID 2969Decanoic AcidHCID 71204Apovincamine2×

Product 1

HCID 86736098HCID 86736098, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

According to the preceding example, 4.5 g of the salt are prepared, starting from 3.36 g (10-2 moles) of apovincamine and 1.72 g (10-2 moles) of capric acid. The product is a semisolid, low melting substance, insoluble in water and alcohol, with an apovincamine content of 50%.

Workup

  1. customare prepared

Sources & evidence

ORD record
ord-1079eed7e829479a80fdada9c5d32afc
Source dataset
uspto-grants-1978_10
Patent number
US04122179

Reaction notes

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