Acetic Anhydride → HCID 12556876, compound

HRID 1112390Notes

Reaction equation

HRID 1112390 reaction equation
[CH2:1]([NH:5][C:6]1[O:7][CH:8]=[C:9]([CH3:11])[N:10]=1)[CH2:2][CH2:3][CH3:4].[C:12](OC(=O)C)(=[O:14])[CH3:13]>>[CH2:1]([N:5]([C:6]1[O:7][CH:8]=[C:9]([CH3:11])[N:10]=1)[C:12](=[O:14])[CH3:13])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 122952262-Oxazolamine, N-butyl-4-methyl-

Product 1

HCID 12556876HCID 12556876, compoundYield 75.4%

Procedure

The procedure of Example 17 was followed using 15.0 g. (0.0974 m) of 2-butylamino-4-methyl oxazole and 25 c.c. of acetic anhydride. B.p. = 58°-60° C/0.1 mm. wt. = 14.4 g. yield = 75.4%.

Sources & evidence

ORD record
ord-fd7f8e272df741419b11543629ca6706
Source dataset
uspto-grants-1978_10
Patent number
US04122183

Reaction notes

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