反应详情

The dried ether solution of 1-amino-3,5-dimethyl-adamantane was treated with 0.5 gram concentrated sulfuric acid (H2SO4) in an ice bath, shaken, and the ether distilled. The oily residue was crystallized from hot water. Yield: 1.81 grams (80% of the theoretical yield).

1. distillationthe ether distilled
2. customThe oily residue was crystallized from hot water
3. customYield: 1.81 grams (80% of the theoretical yield)