HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyltriphenylphosphonium bromide → 6-Methoxy-2-[2-phenylethenyl]-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyltriphenylphosphonium bromide | HCID 2734970 | — |
| Reactant | 6-Methoxy-1H-indole-2-carbaldehyde | HCID 21980688 | — |
| Product | 6-Methoxy-2-[2-phenylethenyl]-1H-indole | HCID 73123140 | 94% |
Reaction Steps
Reaction of 6-methoxyindole-2-carboxaldehyde (145) with benzyltriphenylphosphonium bromide using the procedure described in example 37 gave (146) (94%) as a white solid (mixture of E/Z isomers) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094798B1 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-44e17ed999e24f12a40be8ec409048b0 |
| Source note | uspto-grants-2006_08 |