HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → N,N-Dimethyl-3-[2-[[(phenylmethyl)imino]methyl]phenoxy]propanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 2-[3-(Dimethylamino)propoxy]benzaldehyde | HCID 2995968 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N,N-Dimethyl-3-[2-[[(phenylmethyl)imino]methyl]phenoxy]propanamine | HCID 20394039 | — |
Reaction Steps
A solution of 20.0 g of 2-(3-dimethylaminopropoxy)-benzaldehyde and 10.3 g of benzylamine in 100 ml of toluene is heated at reflux for 1 hour in a procedure described for Example 1. The yield of product is 22.1 g, boiling point 175°-178° C/0.05 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04122255 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-37b97694ba1848bba94a7fe99df6e7a5 |
| Source note | uspto-grants-1978_10 |