2-Piperidino-4-imino-2-thiazoline hydrochloride → HCID 178479155, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][C:10]=1[Cl:11])[C:7](=[NH:12])[NH:6][C:5]2=N.Cl.[C:15]1([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][NH:26][C:27]2[S:28][CH2:29][C:30](=[NH:32])[N:31]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.Cl.N1(C2SCC(=N)N=2)CCCCC1>>[ClH:1].[NH:12]=[C:7]1[C:8]2[C:4](=[CH:3][C:2]([Cl:1])=[C:10]([Cl:11])[CH:9]=2)[C:5](=[C:29]2[S:28][C:27]([NH:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[N:31][C:30]2=[NH:32])[NH:6]1Participants
4
Procedure
Following the procedure described in Example 9, part B above but using equivalent amounts of 5,6-dichloro-1,3-diiminoisoindoline and 2-(5-phenylpentylamino)-4-imino-2-thiazoline hydrochloride in place of the 1,3-diiminoisoindoline and 2-piperidino-4-imino-2-thiazoline hydrochloride respectively, there is obtained as the product 1-imino-5,6-dichloro-3-[2-(5-phenylpentylamino)-4-imino-2-thiazolin-5-ylidene]isoindoline hydrochloride.
Sources & evidence
- ORD record
- ord-ae0360c56755497581fb06540af8aab5
- Source dataset
- uspto-grants-1978_10
- Patent number
- US04122261
Reaction notes
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