HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → Fenvalerate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| Reactant | 2-(4-Chlorophenyl)-3-methylbutanoyl chloride | HCID 4178001 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | Fenvalerate | HCID 3347 | — |
Reaction Steps
A 500 ml round-bottomed flask equipped with a paddle stirrer was charged with 100 mmol of 3-phenoxybenzaldehyde, 100 mmol of 2-(4-chlorophenyl)-3-methylbutanoyl chloride, 120 mmol of sodium cyanide, 10 ml of water, and 200 ml of n-heptane. The molar ratio of water to sodium cyanide was 4.64, all NaCN being dissolved. The mixture thus formed was stirred and analysed. Table VI presents the yields and purities of the desired ester after the reaction time indicated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04123451 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-dced4548778d4b5fbc68b4a165a71eaa |
| Source note | uspto-grants-1978_10 |