Ethylene Oxide → HCID 22762603, compound
Reaction equation
[C:1]1([C:7]2[S:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:12]1[O:14][CH2:13]1>>[C:1]1([C:7]2[S:8][C:9]([CH2:12][CH2:13][OH:14])=[CH:10][CH:11]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1Participants
3
Procedure
2-Phenylthiophene(16.0g;0.1 mole) was reacted in a similar manner to Example 40 but using ethylene oxide (10ml; 0.2 mole) instead of paraformaldehyde. The title compound was obtained as a pale yellow crystalline solid, m.p. 74° C.
Sources & evidence
- ORD record
- ord-ae5bbab9570e4177bd1436d020fcb01d
- Source dataset
- uspto-grants-1978_10
- Patent number
- US04123529
Reaction notes
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