Triethylamine → HCID 22762680, compound

Participants

Reaction Steps

The product from (b) (2.9g;0.009 mole) was stirred in anhydrous ether (50ml) at room temperature and reacted with methanesulphonyl chloride (0.68ml) in the presence of triethylamine (1.2ml). The mixture was stirred overnight, then the ether was evaporated to give a solid which was partitioned between water/chloroform. The chloroform extract was washed with saturated sodium chloride solution and evaporated to give the desired compound as a highly crystalline solid which was recrystallised from ethyl acetate, m.p. 178° C.

Provenance & Evidence