HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Chloromethoxy)-2-methoxyethane → Methyl 4-[7-(1-adamantyl)-6-methoxyethoxymethoxy-2-naphthyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Chloromethoxy)-2-methoxyethane | HCID 77590 | — |
| Reactant | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| Product | Methyl 4-[7-(1-adamantyl)-6-methoxyethoxymethoxy-2-naphthyl]benzoate | HCID 70230892 | 55% |
Reaction Steps
Following the basic procedure of Example 12, by reacting 980 mg (2.4 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 330 μl (28.6 mmol) of methoxyethoxymethyl chloride, 650 mg (55%) of the expected compound were obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723499 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-9a85735f44d44b4dad4458afbbf407f8 |
| Source note | uspto-grants-1998_03 |