HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boronic Acid → 7-(1-Adamantyl)-6-tert-butyldimethylsilyloxy-2-naphthylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boronic Acid | HCID 61668 | — |
| Reactant | 7-(1-Adamantyl)-6-tert-butyldimethylsilyloxy-2-bromonaphthalene | HCID 19694681 | — |
| Product | 7-(1-Adamantyl)-6-tert-butyldimethylsilyloxy-2-naphthylboronic acid | HCID 19694665 | — |
Reaction Steps
Following the basic procedure of Example 7(e), beginning with 11.9 g (25.4 mmol) of 7-(1-adamantyl)-6-tert-butyldimethylsilyloxy-2-bromonaphthalene, 8.37 g (75%) of the expected boronic acid of melting point 221°-222° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723499 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-3150c5b19251400f94abae6bc2510c0b |
| Source note | uspto-grants-1998_03 |