HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 13216997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | HCID 374052 | HCID 374052 | — |
| Product | HCID 13216997 | HCID 13216997 | — |
Reaction Steps
15 parts of 2-methyl-5H-thiazolo[2,3-b]quinazolin-5-one were introduced slowly into 70 parts of chlorosulfonic acid, at 20°-30° C. Stirring was continued for 12 hours, and the 2-methyl-7-chlorosulfonyl-5H-thiazolo[2,3-b]quinazolin-5-one formed was precipitated with ice water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04486221 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-bb11604a97f74a52b56d810621b252a9 |
| Source note | uspto-grants-1984_12 |