HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 4-(4-morpholinyl)- → HCID 178418945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 4-(4-morpholinyl)- | HCID 75655 | — |
| Reactant | HCID 178418992 | HCID 178418992 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178418945 | HCID 178418945 | — |
Reaction Steps
The named compound is prepared by refluxing 0.020 gms E & Z 3-hydroxymethylene-6-(3-methoxy-phenyl)-1,3-dihydro-indol-2-one with 0.020 gms. 4-morpholin-4-yl-phenylamine in tetrahydrofuran (0.33 mL) for 2 days. Following cooling to room temperature, solvent evaporation in vacuo, trituration with isopropanol and filtration the reaction yields the named compound as a solid in the amount of 15.7 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07098236B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-e83cfed6237146ecaad1c4492e25a9ff |
| Source note | uspto-grants-2006_08 |