Caprolactam → HCID 178516026, compound

HRID 1154013Notes

Reaction equation

HRID 1154013 reaction equation
C([Mg:3][Br:4])C.[C:5]1(=[O:12])[NH:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1>C(OCC)C>[C:5]1(=[O:12])[NH:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1.[Br:4][Mg:3]

Participants

4

Reactant 2

HCID 7768CaprolactamHCID 178418443HCID 178418443, compound

Product 1

HCID 178516026HCID 178516026, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

At the same time a solution of bromomagnesium caprolactam was prepared from a mixture of 20.6 mL of ethyl magnesium bromide, 2.0 molar in ethyl ether, and 104.74 q of caprolactam.

Sources & evidence

ORD record
ord-56b0606c505643b6a950bd38efff8459
Source dataset
uspto-grants-1984_12
Patent number
US04487920

Reaction notes

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