Hydrochloric Acid → HCID 73665701, compound

Participants

Reaction Steps

The procedure is carried out in the manner described in Example 1(b) but with the use of 110 g (0.5 mol) of 3,3,12,12-tetramethyl-1-aza-1,5,9-cyclododecatriene, 41 g (0.25 mol) of hydroxylamine sulfate, 50 ml of concentrated hydrochloric acid and 250 ml of water. There is obtained on distillation 85 g (0.337 mol) of 2,2,11,11-tetramethyl-11-amino-undeca-4,8-dienal-oxime; yield 67.4% of theory; b.p. 130° C./7 Pa.

Provenance & Evidence