Sodium Hydroxide → HCID 178485099, compound

HRID 1154288Notes

Reaction equation

HRID 1154288 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH:13][CH3:14])=[NH:12].[OH-].[Na+]>>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH:13][CH3:14])=[NH:12]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 178485100HCID 178485100, compound

Product 1

HCID 178485099HCID 178485099, compound

Procedure

The free base is prepared by dissolving 1-(2,6-dichlorophenyl)-3-methylguanidine hydrochloride to 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 1-(2,6-dichlorophenyl)-3-methylguanidine.

Workup

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

Sources & evidence

ORD record
ord-a24394e57249473ba5913ff207652a72
Source dataset
uspto-grants-1984_12
Patent number
US04488993

Reaction notes

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