1,3-Propanediamine → HCID 20434879, compound

Participants

Reaction Steps

A mixture of 4-vinylpyridine (10.8 cm3), 1,3-diaminopropane (25 cm3) and "Triton B" (Trade Mark) (5 g; 40% solution in water) was stirred and heated at 130° for 20 hours. Water (100 cm3) was added and the mixture was extracted with chloroform (3×100 cm3). The dried (MgSO4) extracts were evaporated in vacuo to give an oil which was distilled to give 5.4 g of N-[2-(4-pyridyl)ethyl]-1,3-diaminopropane as an oil, b.p. 150°/0.03 mm. (Kugelrohr).

Provenance & Evidence