5-Chlorothiophene-2-carbonyl Chloride → HCID 13371096, compound

HRID 1154340Notes

Reaction equation

HRID 1154340 reaction equation
[CH3:1][CH:2]([N:6]1[CH:10]=[CH:9][N:8]=[CH:7]1)[CH2:3][CH2:4][NH2:5].[Cl:11][C:12]1[S:16][C:15]([C:17](Cl)=[O:18])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[S:16][C:15]([C:17]([NH:5][CH2:4][CH2:3][CH:2]([N:6]2[CH:10]=[CH:9][N:8]=[CH:7]2)[CH3:1])=[O:18])=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 5892235-Chlorothiophene-2-carbonyl ChlorideHCID 139528623-(1H-Imidazol-1-yl)butan-1-amine

Product 1

HCID 13371096HCID 13371096, compound

Procedure

When gamma-methyl-1H-imidazole-1-propanamine is treated with 5-chlorothiophene-2-carbonyl chloride by the procedure of Example 36, the above compound, m.p. 141°-143° C., is obtained.

Workup

  1. customthe above compound, m.p. 141°-143° C., is obtained

Sources & evidence

ORD record
ord-c4ad8fd63f9145aeb3a9f04032ea39d1
Source dataset
uspto-grants-1984_12
Patent number
US04489089

Reaction notes

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