HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 2-Oxahexyl-p-methoxybenzene sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 4-Methoxybenzenesulfonic acid | HCID 604723 | — |
| Reactant | 1-Diazoniohex-1-en-2-olate | HCID 54437629 | — |
| Product | 2-Oxahexyl-p-methoxybenzene sulfonate | HCID 20435333 | 70.3% |
Reaction Steps
A 1.0 g quantity of 1-diazo-2-hexanone is dissolved in 50 ml of ether, and 2.5 g of p-methoxybenzenesulfonic acid is slowly added to the solution at room temperature. The same procedure as in Example 1 is thereafter repeated to afford 1.6 g of 2-oxahexyl-p-methoxybenzene sulfonate in the form of a colorless transparent oil (Compound 35). Yield 70.3%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04489091 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-69b63e306c334b90b612b068c5197936 |
| Source note | uspto-grants-1984_12 |