Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Mesitylenesulfonic acid dihydrate → HCID 12821698, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Mesitylenesulfonic acid dihydrate | HCID 15620344 | — |
| 반응물 | HCID 54456867 | HCID 54456867 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 12821698 | HCID 12821698 | 69% |
반응 단계
A 1.0 g quantity of 1-diazo-2-nonanone is dissolved in 30 ml of ether, and 2.0 g of 2,4,6-trimethylbenzenesulfonic acid dihydrate is slowly added to the solution at room temperature. The same procedure as in Example 1 is thereafter repeated to give 1.4 g of 2-oxononanyl-2,4,6-trimethylbenzene sulfonate in the form of a colorless transparent oil (Compound 77). Yield 69.0%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04489091 |
| 출처 데이터셋 | uspto-grants-1984_12 |
| ORD ID | ord-977694975ef24401aac9f577832f021a |
| 출처 메모 | uspto-grants-1984_12 |