HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bisulfite → HCID 20264094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bisulfite | HCID 104748 | — |
| Reactant | (Z)-3-(prop-2-enylcarbamoyl)prop-2-enoic acid | HCID 1551409 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20264094 | HCID 20264094 | — |
Reaction Steps
Allylamine reacts readily with maleic anhydride in THF to give N-allylmaleamic acid (VIII) in quantitative yield. VIII reacts with bisulfite in water to form 3-carboxy-3-sulfo-N-allyl propionamide (IX). At 160° C., (IX) cyclolyzes slowly to form N-allyl-sulfo-succinimide (X).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04490308 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-edf43e089f024aeeb162a30c8bbe113a |
| Source note | uspto-grants-1984_12 |