Phenylacetic Acid → HCID 86739853, compound

Participants

Reaction Steps

To a solution of 1.4 g of phenylacetic acid in 50 ml of dried pyridine, was added 3.1 g of DCC. After 30 minutes of stirring, 2.6 g of 4-(β-amidinoethenyl)phenol methanesulfonate was added to the mixture and stirred overnight. The insolubles were removed by filtration and ethyl ether was added to the filtrate to precipitate crystals. The crystals were collected by filtration and recrystallized from ethanol to obtain 1.5 g of 4-(β-amidinoethenyl)phenyl phenylacetate methanesulfonate.

Provenance & Evidence