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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1154613Generated: October 26, 2026

Dimethyl Sulfoxide → alpha-(alpha-Methyl-3,4-dimethoxyphenethylimino)-2-methoxyacetophenone

https://huagongshe.com/reaction/1154613

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfoxideHCID 679—
Reactant(+-)-3,4-DimethoxyamphetamineHCID 8423—
Reactant2-Methoxyphenylglyoxal hydrateHCID 20434110—
Productalpha-(alpha-Methyl-3,4-dimethoxyphenethylimino)-2-methoxyacetophenoneHCID 20434111—

Reaction Steps

4.9 g of 2-methoxyphenylglyoxal hydrate (crude oil) are dissolved in 15 ml of dimethylsulfoxide, and 5.25 g of α-methyl-3,4-dimethoxyphenethylamine are added thereto. The mixture is stirred at room temperature for 30 minutes, whereby a solution of α-(α-methyl-3,4-dimethoxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04490392
Source datasetuspto-grants-1984_12
ORD IDord-6973e76364714f72973d1babc2791eba
Source noteuspto-grants-1984_12