HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 20434109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | (+-)-p-Methoxyamphetamine | HCID 31721 | — |
| Reactant | 2-Methoxyphenylglyoxal hydrate | HCID 20434110 | — |
| Product | HCID 20434109 | HCID 20434109 | — |
Reaction Steps
2.9 g of 2-methoxyphenylglyoxal hydrate (crude oil) are dissolved in 6 ml of dimethylsulfoxide, and 2 g of α-methyl-4-methoxyphenethylamine are added thereto. The mixture is treated in the same manner as described in Example 1-(2), whereby a solution of α-(α-methyl-4-methoxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04490392 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-0932d662c2e9447a9a8418898ede9ca9 |
| Source note | uspto-grants-1984_12 |