HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 86739855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | 3,4-Methylenedioxyamphetamine | HCID 1614 | — |
| Reactant | 2-Methoxyphenylglyoxal hydrate | HCID 20434110 | — |
| Product | HCID 86739855 | HCID 86739855 | — |
Reaction Steps
5 g of 2-methoxyphenylglyoxal hydrate (crude oil) are dissolved in 15 ml of dimethylsulfoxide, and 4.83 g of α-methyl-3,4-methylenedioxyphenethylamine are added thereto. The mixture is treated in the same manner as described in Example 1-(2), whereby a solution of α-(α-methyl-3,4-methylenedioxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04490392 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-66ad69158e4d454cb730734fdb3c2f3b |
| Source note | uspto-grants-1984_12 |