HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13520695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3,4-Dimethoxy-1,2-benzenediacetonitrile | HCID 10036245 | — |
| Product | HCID 13520695 | HCID 13520695 | — |
Reaction Steps
3.7 gm (0.017 mol) of 3,4-dimethoxy-o-phenylenediacetonitrile were suspended in 10 ml of glacial acetic acid, and the suspension was mixed at 20° C. with 12 ml of 30% hydrobromic acid in glacial acetic acid. After stirring for 3 hours at room temperature, the obtained precipitate was suction-filtered off, washed with glacial acetic acid and then with acetone/ether, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04490369 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-9581e0427ced4d40824bf52f8f3bcd38 |
| Source note | uspto-grants-1984_12 |