4-Methoxy-N-methylbenzeneethanamine → HCID 20433841, compound

HRID 1154642Notes

Reaction equation

HRID 1154642 reaction equation
[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14][Cl:15])[CH:10]=[CH:11][C:5]=2[CH:4]=1.[CH3:21][NH:22][CH2:23][CH2:24][C:25]1[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[CH:27][CH:26]=1>>[ClH:15].[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14][N:22]([CH3:21])[CH2:23][CH2:24][C:25]3[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[CH:27][CH:26]=3)[CH:10]=[CH:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 1047354-Methoxy-N-methylbenzeneethanamineHCID 130925033-(3-Chloropropyl)-1,3-dihydro-7,8-dimethoxy-2H-3-benzazepin-2-one

Product 1

HCID 20433841HCID 20433841, compound

Procedure

This compound was prepared analogous to Example 1(b) by reacting 1-(7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-3-chloropropane with N-methyl-N-[2-(4-methoxy-phenyl)-ethyl]-amine.

Workup

  1. customThis compound was prepared analogous to Example 1(b)

Sources & evidence

ORD record
ord-3416e3338e6943d3a2916bec3649b804
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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