N-Methylhomoveratrylamine → HCID 20433724, compound

HRID 1154645Notes

Reaction equation

HRID 1154645 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][Cl:16])[C:9](=[O:17])[CH2:8][C:7]=2[CH:18]=1.[CH3:19][NH:20][CH2:21][CH2:22][C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[C:25]([O:31][CH3:32])[CH:24]=1>>[ClH:16].[ClH:16].[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][N:20]([CH3:19])[CH2:21][CH2:22][C:23]3[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[C:25]([O:31][CH3:32])[CH:24]=3)[C:9](=[O:17])[CH2:8][C:7]=2[CH:18]=1

Participants

3

Reactant 2

HCID 77039N-MethylhomoveratrylamineHCID 137469313-(3-Chloropropyl)-1,3,4,5-tetrahydro-8-methoxy-2H-3-benzazepin-2-one

Product 1

HCID 20433724HCID 20433724, compound

Procedure

This compound was prepared analogous to Example 5(b) by reaction of 1-(8-methoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-3-chloro-propane with N-methyl-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-amine.

Sources & evidence

ORD record
ord-21d2308fd2724de5820cddcbfa6a349d
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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