1-Bromo-2-Chloroethane → HCID 20433680, compound
Reaction equation
[CH3:1][O:2][C:3]1[C:14]([O:15][CH3:16])=[CH:13][C:6]2[CH2:7][C:8](=[O:12])[NH:9][CH:10]=[CH:11][C:5]=2[CH:4]=1.[Cl:17][CH2:18][CH2:19]Br>>[CH3:1][O:2][C:3]1[C:14]([O:15][CH3:16])=[CH:13][C:6]2[CH2:7][C:8](=[O:12])[N:9]([CH2:19][CH2:18][Cl:17])[CH:10]=[CH:11][C:5]=2[CH:4]=1Participants
3
Procedure
This compound was prepared analogous to Example 1(a) by reacting 7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one with 1-chloro-2-bromo-ethane.
Workup
- customThis compound was prepared analogous to Example 1(a)
Sources & evidence
- ORD record
- ord-c97187e04f2f410cb4cfd854a587660c
- Source dataset
- uspto-grants-1984_12
- Patent number
- US04490369
Reaction notes
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