N-Methylhomoveratrylamine → HCID 20433753, compound

HRID 1154659Notes

Reaction equation

HRID 1154659 reaction equation
[CH3:1][O:2][C:3]1[C:19]([O:20][CH3:21])=[CH:18][C:6]2[CH2:7][C:8](=[O:17])[N:9]([CH2:13][CH2:14][CH2:15][Cl:16])[C:10](=[O:12])[CH2:11][C:5]=2[CH:4]=1.[CH3:22][NH:23][CH2:24][CH2:25][C:26]1[CH:31]=[CH:30][C:29]([O:32][CH3:33])=[C:28]([O:34][CH3:35])[CH:27]=1>>[ClH:16].[CH3:1][O:2][C:3]1[C:19]([O:20][CH3:21])=[CH:18][C:6]2[CH2:7][C:8](=[O:17])[N:9]([CH2:13][CH2:14][CH2:15][N:23]([CH3:22])[CH2:24][CH2:25][C:26]3[CH:31]=[CH:30][C:29]([O:32][CH3:33])=[C:28]([O:34][CH3:35])[CH:27]=3)[C:10](=[O:12])[CH2:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 77039N-MethylhomoveratrylamineHCID 20433817HCID 20433817, compound

Product 1

HCID 20433753HCID 20433753, compound

Procedure

This compound was prepared analogous to Example 5(b) by reacting 1-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepine-2,4-dione-3-yl)-3-chloro-propane with N-methyl-N[2-(3,4-dimethoxy-phenyl)-ethyl]-amine.

Workup

  1. customThis compound was prepared analogous to Example 5(b)

Sources & evidence

ORD record
ord-6b2e9e4f59d7409696af2ac07ab429be
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

Loading…