N-Methylhomoveratrylamine → HCID 20433723, compound

HRID 1154662Notes

Reaction equation

[OH:1][C:2]1[C:17]([O:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:16][C:5]2[CH2:6][C:7](=[O:15])[N:8]([CH2:11][CH2:12][CH2:13]Cl)[CH2:9][CH2:10][C:4]=2[CH:3]=1.[CH3:26][NH:27][CH2:28][CH2:29][C:30]1[CH:35]=[CH:34][C:33]([O:36][CH3:37])=[C:32]([O:38][CH3:39])[CH:31]=1>>[OH:1][C:2]1[C:17]([O:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:16][C:5]2[CH2:6][C:7](=[O:15])[N:8]([CH2:11][CH2:12][CH2:13][N:27]([CH3:26])[CH2:28][CH2:29][C:30]3[CH:35]=[CH:34][C:33]([O:36][CH3:37])=[C:32]([O:38][CH3:39])[CH:31]=3)[CH2:9][CH2:10][C:4]=2[CH:3]=1

Participants

Reactant 2

HCID 77039N-Methylhomoveratrylamine

HCID 20433700HCID 20433700, compound

Product 1

HCID 20433723HCID 20433723, compound

Procedure

This compound was prepared analogous to Example 5(b) by reacting 1-(7-hydroxy-8-benzyloxy-1,3,4,5-tetrahydro-2-H-3-benzazepin-2-on-3-yl)-3-chloro-propane with N-methyl-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-amine.

Workup

customThis compound was prepared analogous to Example 5(b)

Sources & evidence

ORD record: ord-fa037b8d2c184c83a008590b8859f293
Source dataset: uspto-grants-1984_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04490369

Reaction notes

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