N-Methylhomoveratrylamine → 1-[7,8-Dimethyl-1,3-dihydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{3,4-dimethoxy-phenyl}ethyl)-amino]-propane hydrochloride

HRID 1154666Notes

Reaction equation

HRID 1154666 reaction equation
[CH3:1][C:2]1[C:17]([CH3:18])=[CH:16][C:5]2[CH2:6][C:7](=[O:15])[N:8]([CH2:11][CH2:12][CH2:13][Cl:14])[CH:9]=[CH:10][C:4]=2[CH:3]=1.[CH3:19][NH:20][CH2:21][CH2:22][C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[C:25]([O:31][CH3:32])[CH:24]=1>>[ClH:14].[CH3:1][C:2]1[C:17]([CH3:18])=[CH:16][C:5]2[CH2:6][C:7](=[O:15])[N:8]([CH2:11][CH2:12][CH2:13][N:20]([CH3:19])[CH2:21][CH2:22][C:23]3[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[C:25]([O:31][CH3:32])[CH:24]=3)[CH:9]=[CH:10][C:4]=2[CH:3]=1

Participants

3

Reactant 2

HCID 77039N-MethylhomoveratrylamineHCID 204337661-(7,8-Dimethyl-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-3-chloro-propane

Product 1

HCID 204336741-[7,8-Dimethyl-1,3-dihydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{3,4-dimethoxy-phenyl}ethyl)-amino]-propane hydrochloride

Procedure

This compound was prepared analogous to Example 1(b) by reacting 1-(7,8-dimethyl-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-3-chloro-propane with N-methyl-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-amine.

Workup

  1. customThis compound was prepared analogous to Example 1(b)

Sources & evidence

ORD record
ord-2484ed13b7464288a3993404dc788186
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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