N-Methylhomoveratrylamine → HCID 20433727, compound

HRID 1154668Notes

Reaction equation

HRID 1154668 reaction equation
[CH3:1][O:2][C:3]1[C:19]([O:20][CH3:21])=[CH:18][C:6]2[CH2:7][C:8](=[O:17])[N:9]([CH2:12][CH:13]([CH3:16])[CH2:14]Cl)[CH:10]=[CH:11][C:5]=2[CH:4]=1.[CH3:22][NH:23][CH2:24][CH2:25][C:26]1[CH:31]=[CH:30][C:29]([O:32][CH3:33])=[C:28]([O:34][CH3:35])[CH:27]=1>>[CH3:1][O:2][C:3]1[C:19]([O:20][CH3:21])=[CH:18][C:6]2[CH2:7][C:8](=[O:17])[N:9]([CH2:12][C:13]([CH3:16])([N:23]([CH3:22])[CH2:24][CH2:25][C:26]3[CH:31]=[CH:30][C:29]([O:32][CH3:33])=[C:28]([O:34][CH3:35])[CH:27]=3)[CH3:14])[CH:10]=[CH:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 77039N-MethylhomoveratrylamineHCID 20433668HCID 20433668, compound

Product 1

HCID 20433727HCID 20433727, compound

Procedure

This compound was prepared analogous to Example 1(b) by reacting 1-(7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-2-methyl-3-chloro-propane with N-methyl-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-amine.

Workup

  1. customThis compound was prepared analogous to Example 1(b)

Sources & evidence

ORD record
ord-960c32d0d6874251855c8a668f7b8aa4
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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