HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → 1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-1,2-dione-3-yl]-3-[N-methyl-N-(2-{4-amino-3,5-dichloro-phenyl}-ethyl)-amino]-propane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4-amino-3,5-dichloro-phenyl}-ethyl)-amino]-propane | HCID 13316678 | — |
| Product | 1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-1,2-dione-3-yl]-3-[N-methyl-N-(2-{4-amino-3,5-dichloro-phenyl}-ethyl)-amino]-propane | HCID 20433667 | — |
Reaction Steps
This compound was prepared analogous to Example 5(b) from 1-[7,8dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin- 2-on-3-yl]-3-[N-methyl-N-(2-{4-amino-3,5-dichloro-phenyl}-ethyl)-amino]-propane and selenium dioxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04490369 |
| Source dataset | uspto-grants-1984_12 |
| ORD ID | ord-ba6162a6a5134a1c8b4d7ed70e2b983a |
| Source note | uspto-grants-1984_12 |