N-Methylbenzeneethanamine → HCID 13319936, compound

HRID 1154679Notes

Reaction equation

HRID 1154679 reaction equation
[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14][Cl:15])[CH2:10][CH2:11][C:5]=2[CH:4]=1.[CH3:21][NH:22][CH2:23][CH2:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[ClH:15].[ClH:15].[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14][N:22]([CH3:21])[CH2:23][CH2:24][C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 11503N-MethylbenzeneethanamineHCID 130925103-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

Product 1

HCID 13319936HCID 13319936, compound

Procedure

This compound was prepared analogous to Example 5(b) by reacting 1-[7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-chloropropane with N-methyl-2-phenyl-ethylamine.

Workup

  1. customThis compound was prepared analogous to Example 5(b)

Sources & evidence

ORD record
ord-d72218283fa149f6935fc023bfcd05b2
Source dataset
uspto-grants-1984_12
Patent number
US04490369

Reaction notes

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