Toluene → HCID 20563292, compound

Participants

Reaction Steps

36.8 g (0.2 mole) of p-aminodiphenylamine was added to 200 ml of toluene, and 16.8 g of sodium hydrogen carbonate and 30 ml of water was added. With stirring, 30.5 g (0.2 mole) of p-chloromethylstyrene was added dropwise to the mixture at 60° C. After the addition, the mixture was stirred at less than 60° C. for 4 hours. The resulting precipitate was separated, and washed with water to afford 49.8 g (yield 83%) of 4-anilino-N-(4-vinylbenzyl)aniline having a melting point of 143° C.

Provenance & Evidence