Octanoic Acid → 2-Imidazoline, 2-heptyl-

HRID 1154904Notes

Reaction equation

[C:1](O)(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:11]([NH2:14])[CH2:12][NH2:13]>>[CH2:2]([C:1]1[NH:13][CH2:12][CH2:11][N:14]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 2

HCID 379Octanoic Acid

HCID 3301Ethylenediamine

Product 1

HCID 315302-Imidazoline, 2-heptyl-Yield 95%

Procedure

The procedure described in Example 5 is followed except that 288 parts of n-octanoic acid and 132 parts of ethylenediamine are employed. 319 parts of 2-n-heptylimidazoline (95% of theory, based on octanoic acid employed) of boiling point 133° C./5.32 mbar are obtained.

Sources & evidence

ORD record: ord-ec982ac59ec1479c9558892ccceaa57c
Source dataset: uspto-grants-1981_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04298748

Reaction notes

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