HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 77456-46-3
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1H-Purine, 8-(4-methoxy-2-(2-(methylthio)ethoxy)phenyl)- | HCID 3059914 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | 77456-46-3 | HCID 3059915 | — |
Reaction Steps
One gram of 8-[4-methoxy-2-(2-methylmercapto-ethoxy)phenyl]purine was dissolved in 10 ml of glacial acetic acid and mixed with 0.5 ml of 30% hydrogen peroxide. After standing for 3.5 hours at room temperature, the reaction mixture was diluted with water and made alkaline by means of potassium carbonate. The precipitate was recrystallized from isopropanol/ethanol in a volume ratio of 1:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04299834 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-04319949ba4f417380491cc005a4805d |
| Source note | uspto-grants-1981_11 |