反应详情

温度

60 °C

A 2.5 ml portion of the above prepared bistrimethylsilyl-3-cyanopropylphosphonate solution in CCl4 was added dropwise 0.049 g of zirconium tetra propoxide. The reaction mixture was heated to 60° C. and filtered. The filtrate was saved. About 0.058 g of zirconium-3-cyanopropylphosphonate was formed.

1. filtrationfiltered